6–11 Jul 2014
Palazzo del Bo and Centro Culturale San Gaetano, Padova
Europe/Rome timezone

P46 - Searching for Late Bronze Age soldering techniques: µPIXE analyses of the gold bracelets from Herdade do Álamo (Beja, Portugal)

11 Jul 2014, 13:00
1h
Palazzo del Bo and Centro Culturale San Gaetano, Padova

Palazzo del Bo and Centro Culturale San Gaetano, Padova

Board: 46

Speaker

Dr Luis Alves (C2TN, IST/CTN, Universidade de Lisboa, E.N. 10, 2686-953 Sacavém, Portugal)

Description

Several technological changes emerged in the Atlantic façade of the Iberian Peninsula during the Late Bronze Age. Goldwork gained new forms by joining hollow casted pieces. Two bracelets from the collection of the National Archaeological Museum in Lisbon, produced by joining 10 round sections solid casted thin rings, are the most representative gold items of a transition period when the ancient solid casting techniques are used simultaneously with the new techniques. No analytical study was carried out on the very rare objects representative of this transition period. In this work we present the first analytical results obtained for the two bracelets from the find of Herdade do Álamo (Moura, Beja, Portugal) using non-destructive quantitative elemental tecnhiques: portable XRF and µPIXE. Both bracelets were analysed in situ by portable XRF. The equipment comprises an Eclipse IV X-ray source with a Rh anode and a XR-100 SDD Amptek X-ray detector at 90º geometry. The identification of the joining technology requiring higher spatial resolution was carried out through µPIXE analysis using a 2 MeV proton beam focused down to 100x100 µm2 at the external microbeam setup of the IST/ITN van de Graff accelerator comprised of a OM150 quadrupole triplet system and a 30 mm2 Bruker SDD X-ray detector. The results indicate that the solid thin rings were produced with two different alloys with an Ag/Au ratio of 0.20 for 12 of the rings and 0.26 for the other 8 rings. The latter show the same composition as the two hollow gold neckrings from the same find, analysed by portable XRF. Micro-PIXE elemental distribution maps and point spectra analysis shows that the bracelets were soldered together using gold alloys with different melting points. Based on this data we could reveal the manufacture technologies employed and propose the first mounting scheme for the bracelets of the Herdade do Álamo find.

Primary author

Isabel Tissot (Universidade de Lisboa Centro de Fisica Atomica and Archeofactu, Lisbon, Portugal)

Co-authors

Dr Luis Alves (C2TN, IST/CTN, Universidade de Lisboa, E.N. 10, 2686-953 Sacavém, Portugal) Maria Filomena Guerra (7 ArchAm - UMR 8096 CNRS, MAE, 21 allée de l’Université, 92023 Nanterre, France) Prof. Maria Luisa Carvalho (Universidade de Lisboa Centro de Fisica Atomica, Lisbon, Portugal) Dr Marta Manso (Centro de Fisica Atomica and Faculdade de Belas-Artes; Universidade de Lisboa, Lisboa, Portugal) Matthias Tissot (2 Archeofactu, Lisbon, Rua do Cerrado das Oliveiras 14, 2Dt, 2610-035, Portugal; 6 Museu Nacional de Arqueologia, Lisbon, Praça do Império, 1400, Portugal) Dr Victoria Corregidor (Campus Tecnológico e Nuclear, Portugal)

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