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This paper reports the results of an experimental investigation to characterize the inner structure of a high-pressure gasoline spray injected by a 6-hole nozzle for Direct Injection Spark Ignition (DISI) engines. A desktop facility based on polycapillary optics system, providing a high flux beam with low divergence has been used. X-ray µ-tomography and radiography measurements in the region just downstream of the nozzle provided the local mass distribution of a single jet. The single-jet fuel mass-rate was obtained and compared with the injection rate one measured by the injection Gauge Rate System working on the Bosch tube principle. The comparison demonstrates the accuracy of x-ray tomography desktop facility as a reliable diagnostic tool.